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    Tandem Wittig-ene reaction approach to kainic acid

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    J_Org_Chem_74_3591.pdf (130.3Kb)
    Date
    2009
    Author
    Majik, M.S.
    Parameswaran, P.S.
    Tilve, S.G.
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    Abstract
    The first example of a tandem Wittig-intramolecular ene reaction approach and its application toward the synthesis of kainic acid is reported. The synthetic pathway involves conversion of prenyl bromide into phosphorane 3, followed by one-pot Wittig olefination and an ene reaction with glyoxalic acid to give the cis fused pyrrolidine skeleton of kainic acid.
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    http://drs.nio.org/drs/handle/2264/3498
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